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Beilstein J. Org. Chem. 2012, 8, 850–860, doi:10.3762/bjoc.8.95
Graphical Abstract
Figure 1: Overview of the DOS strategy.
Scheme 1: Synthesis of linear cyclisation precursors 1–4.
Scheme 2: AlCl3 catalysed tandem Boc-removal/bicyclisation processes; the yields quoted refer to the isolated...
Scheme 3: (a) AlCl3 catalysed formation of tricyclic alkaloid 10 along with an X-ray crystal structure of 10;...
Scheme 4: (a) Optimal conditions to obtain trans-8 and 10 and the control experiments carried out to probe th...
Scheme 5: DOS of 5-5-6 and 5-6-6 tricyclic alkaloids 13 and 14.
Scheme 6: Total synthesis of myrrhine, epi-myrrhine and myrrhine-N-oxide.
Scheme 7: Use of nitromethane in DOS: Synthesis of meso-diphenylpyrrolidizine 17.
Scheme 8: Use of Tris as a substrate for DOS: Synthesis of decorated morpholines 22 and 23.